| 氯虫酰胺的合成与杀虫活性 |
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| 引用本文： | 柴宝山,彭永武,李慧超,张弘,刘长令. 氯虫酰胺的合成与杀虫活性[J]. 农药, 2009, 48(1) |
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| 作者姓名： | 柴宝山 彭永武 李慧超 张弘 刘长令 |
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| 作者单位： | 1. 沈阳化工研究院,沈阳,110021
2. 沈阳化工研究院,沈阳,110021;辽宁大学,沈阳,110036 |
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| 基金项目： | 国家重点基础研究发展规划(973计划)，国家科技支撑计划项目 |
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| 摘 要： | 以2,3-二氯吡啶和2-甲基-4-氯苯胺为起始原料,经过多步反应得到6-氯-2-(3-溴-1-(3-氯吡啶-2-基)-1H-吡唑-5-基)-8-甲基-4H-3,1-苯并嗪-4-酮,再与甲胺反应得到目标产物氯虫酰胺,经核磁验证其结构,生物活性测定结果表明该化合物对鳞翅目害虫如小菜蛾、甜菜夜蛾、稻纵卷叶螟等具有优异的杀虫活性。
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| 关 键 词： | 氯虫酰胺 合成 杀虫活性 |
Synthesis of Chlorantraniliprole and Its Insecticidal Activity |
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| CHAI Bao-shan,PENG Yong-wu,LI Hui-chao,ZHANG Hong,LIU Chang-ling. Synthesis of Chlorantraniliprole and Its Insecticidal Activity[J]. Pesticides, 2009, 48(1) |
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| Authors: | CHAI Bao-shan PENG Yong-wu LI Hui-chao ZHANG Hong LIU Chang-ling |
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| Abstract: | Chlorantraniliprole was synthesized by reacting methylamine with 2-(3-bromo-1-(3-chloropyridin-2-yl)-1H-pyrazol-5-yl)-6-chloro-8-methyl-4H-benzo[d][1,3]oxazin-4-one prepraed from 2,3-dichloropyridine and 4-chloro-2-methylaniline as starting materials via several steps,and its structure was confirmed by 1H NMR.The test results showed that chlorantraniliprole has good activities controlling Plutella xylostella,Laphygma exigua and Chaphalocrocis medina. |
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| Keywords: | chlorantraniliprole synthesis insecticidal activity |
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