| 四氯化锡催化合成除草剂2甲4氯异辛酯 |
| |
| 引用本文： | 朱大顺,魏鹏.四氯化锡催化合成除草剂2甲4氯异辛酯[J].现代农药,2005,4(2):12-13. |
| |
| 作者姓名： | 朱大顺 魏鹏 |
| |
| 作者单位： | 南京苏研科创农化有限公司,南京,211156 |
| |
| 摘 要： | 标题化合物2甲4氯异辛酯由2甲4氯酸和异辛醇在四氯化锡催化作用下合成。将0.05 mol四氯化锡、1 mol 2甲4氯酸、3 mol异辛醇和1000 ml溶剂环己烷,在升温回流带水条件下反应3 h,得到0.9 mol 2甲4氯异辛酯,收率达到90%以上。
|
| 关 键 词： | 催化 合成 四氯化锡 2甲4氯异辛酯 |
| 文章编号： | 1671-5284(2005)02-0012-02 |
| 修稿时间： | 2004年9月15日 |
Catalized Synthesis of MCPA-isoctyl by Stannic Chloride Pentahydrate |
| |
| Zhu Da-shun,Wei Peng.Catalized Synthesis of MCPA-isoctyl by Stannic Chloride Pentahydrate[J].Modern Agrochemicals,2005,4(2):12-13. |
| |
| Authors: | Zhu Da-shun Wei Peng |
| |
| Abstract: | The title compound MCPA-isoctyl was synthesized from MCPA and isoocatnol by SnCl4?5 H2O catalized. The mixture consisted of 0.05 mol SnCl4?5 H2O, 1 mol MCPA, 3 mol isoocatnol and 1 000 ml cyclohexane as solvent was refluxed and dehydrated for 3 hours to give 0.9 mol MCPA-isoctyl in yield of 90% or more. |
| |
| Keywords: | cataliezed synthesis stannic chloride pentahydrate MCPA-isoctyl |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
