| ZnSe微米晶的液相合成及表征 |
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| 引用本文： | 李莉,李天佑.ZnSe微米晶的液相合成及表征[J].辽宁化工,2011,40(6):569-571. |
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| 作者姓名： | 李莉 李天佑 |
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| 作者单位： | 淮南师范学院化学与化工系,安徽淮南,2320011 |
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| 基金项目： | 安徽省2010高校优秀青年人才基金项目,项目号:2010SQRL163 |
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| 摘 要： | 采用液相合成法,实现了多晶硒化锌微米空心球的低温合成。通过扫描电镜选观察到直径在1～4μm左右的ZnSe多晶微米空心球体。用XRD（X射线衍射）测定样品的成分,对样品纯度进行鉴定。用紫外可见光谱对实验样品分析,发现有明显蓝移现象。
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| 关 键 词： | 硒化锌 微米晶 液相合成 |
Liquid-phase Synthesis and Characterization of ZnSe Microcrystal |
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| LI Li,LI Tian-you.Liquid-phase Synthesis and Characterization of ZnSe Microcrystal[J].Liaoning Chemical Industry,2011,40(6):569-571. |
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| Authors: | LI Li LI Tian-you |
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| Affiliation: | LI Li,LI Tian-you(Department of Chemistry and Chemical Engineering,Huainan Normal University.Anhui Huainan 232001,China) |
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| Abstract: | The liquid-synthesis method was used to prepare the micro-hollow-bead of polycrystal ZnSe under relatively low temperature.By the method of scan electron microscope（SEM）,the micro-hollow-bead with 1～4 ？m diameters was observed.By XRD（X-ray Diffraction）,ingredient of the sample was determined,and purity of the sample was identified.Then the sample was analyzed by UV-vis spectrum,the blueshife phenomenon was clearly found. |
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| Keywords: | Zinc selenide Microcrystalline Lquid-synthesis method |
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