Polymethacrylic acid/Na-montmorillonite/SiO2 nanoparticle composites structures and thermal properties |
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Authors: | Yan Bao Jian-zhong Ma |
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Affiliation: | (1) College of Resource and Environment, Shaanxi University of Science and Technology, 710021 Xi’an, China;(2) Key Laboratory of Chemistry and Technology for Light Chemical Industry, Ministry of Education, 710021 Xi’an, China |
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Abstract: | In this article, polymethacrylic acid/Na-montmorillonite/SiO2 nanoparticle (PMAA/Na-MMT/SiO2) composites were prepared via in situ polymerization. Fourier transform infrared spectroscopy (FTIR) indicated that the polymerization of SiO2 nanoparticle and MAA have been taken place. X-ray diffraction (XRD) results suggest that Na-MMT layers are exfoliated during the polymerization process. As evidenced by the transmission electron microscopy (TEM), the Na-MMT layers and SiO2 nanoparticles exhibit good dispersion in the polymer matrix. It was found that the PMAA/Na-MMT/SiO2 composite exhibit considerably enhanced thermal properties compared with the PMAA/Na-MMT. |
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