| 一种新型的功能性氯盐离子液体的制备 |
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| 引用本文： | 张飞雄,张定军,陈玉仙.一种新型的功能性氯盐离子液体的制备[J].应用化工,2010,39(12). |
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| 作者姓名： | 张飞雄 张定军 陈玉仙 |
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| 基金项目： | 甘肃省自然科学基金，兰州市科技计划项目 |
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| 摘 要： | 用咪唑和氯乙酸乙酯合成了1,3-二乙酸乙酯咪唑氯盐离子液体,在75℃下,反应时间为6 h,粗产品用乙腈∶氯仿=1∶1的溶液重结晶,产率可达61%。
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| 关 键 词： | 离子液体 咪唑 氯乙酸乙酯 重结晶 |
The synthesis of a novel functional ionic liquid based chloride |
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| ZHANG Fei-xiong,ZHANG Ding-jun,CHEN Yu-xian.The synthesis of a novel functional ionic liquid based chloride[J].Applied chemical industry,2010,39(12). |
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| Authors: | ZHANG Fei-xiong ZHANG Ding-jun CHEN Yu-xian |
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| Abstract: | 1,3-Di(ethyl acetate) imidazole chloride was synthesized from imidazole and ethyl chloroacetate by chemosynthesis.61% yield was obtained under the reaction conditions:the reaction time 6 h,the reaction temperature 75 ℃,respectively,and the crude product was recrystallized with the blended solvent(Vacetonitrile ∶Vchloroform=1 ∶1). |
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| Keywords: | ionic liquid imidazole ethyl chloroacetate recrystallizations |
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