| 顶空气相色谱-质谱联用法测定卷烟材料中的溶剂残留 |
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| 引用本文： | 朱斌,徐昕荣,向弘,尹诗衡,匡同春.顶空气相色谱-质谱联用法测定卷烟材料中的溶剂残留[J].质谱学报,2010,31(2):116-119. |
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| 作者姓名： | 朱斌 徐昕荣 向弘 尹诗衡 匡同春 |
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| 作者单位： | 华南理工大学分析测试中心，广东 广州510640 |
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| 摘 要： | 采用顶空气相色谱-质谱联用(HS-GC/MS)法测定烟草行业标准YC263-2008卷烟条与包装纸中挥发性有机物溶剂残留,根据物质峰面积和标样浓度,计算回归方程,以及16种溶剂的线性范围、回收率、检出限、精密度等。通过胶粘剂、纸品样的实际检测,验证了方法的可行性,有效避免顶空气相色谱法的干扰问题,顶空气质联用法能准确地检测残留气体。
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| 关 键 词： | 静态顶空 气质联用 溶剂残留 卷烟材料 |
Determination of Residual Solvents in Cigarette Materials by Headspace Gas Chromatography-Mass Spectrometry |
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| ZHU Bin,XU Xin-rong,XIANG Hong,YIN Shi-heng,KUANG Tong-chun.Determination of Residual Solvents in Cigarette Materials by Headspace Gas Chromatography-Mass Spectrometry[J].Journal of Chinese Mass Spectrometry Society,2010,31(2):116-119. |
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| Authors: | ZHU Bin XU Xin-rong XIANG Hong YIN Shi-heng KUANG Tong-chun |
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| Affiliation: | Analytical and Testing Center, South China University of Technology, Guangzhou 510640, China |
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| Abstract: | Total of 16 volatile organic residual solvent compounds in the cigarette paper and the wrapping paper listed in standard YC263-2008 were analyzed by headspace gas chromatography-mass spectrometry(HS-GC/MS).The linear range,recovery rate,precision and detection limit of the 16 residual solvents were tested.The method proved to be successful by the testing results of the adhesive and wrapping paper samples,which can avoid the disturbance problem brought by HS-GC.The results show that HS-GC/MS tests the residu... |
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| Keywords: | static-headspace GC/MS residual solvents cigarette materials |
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