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水杨酸锌配合物的合成及光谱表征
引用本文:申志炜,胡应喜.水杨酸锌配合物的合成及光谱表征[J].北京石油化工学院学报,2012,20(4):58-60.
作者姓名:申志炜  胡应喜
作者单位:北京石油化工学院化学工程学院,北京,102617;北京石油化工学院化学工程学院,北京,102617
摘    要:以氧化锌和水杨酸为原料.用流变相反应法合成了水杨酸锌配合物。通过元素分析确定了该配合物的组成,采用EDTA配位滴定法和AAS法对中心原子锌进行测定,并通过XRD、IR、TG等分析方法对其结构进行了表征。结果表明,该配合物的组成为(HOC5H1CO2)2Zn·3H2O。

关 键 词:水杨酸锌  流变相反应法  合成  表征

The Rheological Phase Synthesis and Spectrum Characterization of Zinc Salicylate
Shen Zhiwei Hu Yingxi.The Rheological Phase Synthesis and Spectrum Characterization of Zinc Salicylate[J].Journal of Beijing Institute of Petro-Chemical Technology,2012,20(4):58-60.
Authors:Shen Zhiwei Hu Yingxi
Affiliation:Shen Zhiwei Hu Yingxi (School of Chemical Engineering,Beijing Institute of Petro-chemical Techmology,Beijing 102617.China)
Abstract:Zinc salicylate complexes are synthesized with the rheological phasereaction method, using zinc oxide and salicylic acid as the raw material.The composition of complex is confirmed by the elemental analysis,and Mn was determined by A AS and EDTA volumetric analysis. XRD,IR and TG/DTA characterize the structure of the product.The experimental result shows the composition of complex is(HOC_6 H_4CO_2 )_2Zn ? 3 H_2O.
Keywords:zinc salicylate  rheological phase  synthesis  characterization
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