| 葡萄糖对苯二酚树脂胶粘剂的合成 |
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| 引用本文： | 陈栓虎,胥学旺,马春平.葡萄糖对苯二酚树脂胶粘剂的合成[J].中国胶粘剂,2007,16(7):28-31. |
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| 作者姓名： | 陈栓虎 胥学旺 马春平 |
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| 作者单位： | 西北大学化学系,陕西,西安,710069 |
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| 摘 要： | 以葡萄糖代替甲醛,在碱性条件下合成了葡萄糖对苯二酚树脂胶粘剂。利用红外光谱(IR)及热重分析(TGA)对树脂的结构及热稳定性进行了分析,并通过正交实验获得了该树脂合成的最佳反应条件:pH=13,n(葡萄糖)n∶(对苯二酚)=101,∶反应温度110℃,催化剂用量2.0%,反应时间7h;同时对树脂的固化条件进行了系统研究。
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| 关 键 词： | D-葡萄糖 对苯二酚 胶粘剂 |
| 文章编号： | 1004-2849（2007）07-0028-04 |
| 修稿时间： | 2007-03-232007-05-14 |
Synthesis of glucose-hydroquinone adhesive |
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| CHEN Shuan-hu,XU Xue-wang,MA Chun-ping.Synthesis of glucose-hydroquinone adhesive[J].China Adhesives,2007,16(7):28-31. |
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| Authors: | CHEN Shuan-hu XU Xue-wang MA Chun-ping |
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| Abstract: | In alkali condition,an adhesive of glucose-hydroquinone resin by using D-glucose instead of formaldehyde was prepared successfully.The structure and thermostability of the resin were characterized by IR and TGA,and through orthogonal experiment the optimum conditions of the reaction were gained:pH = 13,the weight of catalyst is 2.0%(percent of the weight of D-glucose),molar ratio of glucose to hydroquinone is 10∶1,reaction temperature is 110 ℃,reaction time is 7 h.And the curing reaction of the resin was also studied by this method. |
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| Keywords: | D-glucose hydroquinone adhesive |
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