| 相转移催化法合成甲基丙烯酸缩水甘油酯 |
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| 引用本文： | 孙晓云,孔德珍,路国梁,付煜荣.相转移催化法合成甲基丙烯酸缩水甘油酯[J].石油化工,1986(12). |
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| 作者姓名： | 孙晓云 孔德珍 路国梁 付煜荣 |
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| 作者单位： | 河北师范大学 石家庄 |
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| 摘 要： | 以季铵盐为相转移催化剂,由甲基丙烯酸和环氧氯丙烷合成甲基丙烯酸缩水甘油酯。以正交试验法优选出最佳反应时间、温度及催化剂.产品收率为73—87％,纯度为98％。
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Synthesis of Glycidyl Methacrylate by Phase Transfer Catalysis |
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| Abstract: | Glycidyl Methacrylate may be synthesized from methacrylic acid and epichlorohydrin by the process of phase transfer catalysis in the presence of quaternary ammonium salt. The optimum reaction conditions, such as selection of catalysts, reaction time and temperatures were found. The yield was 73—87％. |
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