| 含有酰腙基团的1,3,4-噻二唑衍生物的合成 |
| |
| 引用本文： | 董保东,柳闪星,张谦,朱春风,廖新成.含有酰腙基团的1,3,4-噻二唑衍生物的合成[J].化学试剂,2011(9):795-798,854. |
| |
| 作者姓名： | 董保东 柳闪星 张谦 朱春风 廖新成 |
| |
| 作者单位： | 郑州大学化学系; |
| |
| 摘 要： | 以氨基硫脲为初始原料,合成了5-氨基-1,3,4-噻二唑-2-硫基乙酰肼,再与不同的芳香醛(酮)反应,得到了12个标题化合物.其结构均经IR、1HNMR、13CNMR和MS等测试手段所确认.
|
| 关 键 词： | 酰腙 1 3 4-噻二唑 |
Synthesis 1,3,4-thiadiazole with hydrazones |
| |
| DONG Bao-dong,LIU Shan-xing,ZHANG Qian,ZHU Chun-feng,LIAO Xin-cheng.Synthesis 1,3,4-thiadiazole with hydrazones[J].Chemical Reagents,2011(9):795-798,854. |
| |
| Authors: | DONG Bao-dong LIU Shan-xing ZHANG Qian ZHU Chun-feng LIAO Xin-cheng |
| |
| Affiliation: | DONG Bao-dong,LIU Shan-xing,ZHANG Qian,ZHU Chun-feng,LIAO Xin-cheng(Department of Chemistry,Zhengzhou University,Zhengzhou 450052,China) |
| |
| Abstract: | A series of acylhydrazones with 1,3,4-thiadiazole were synthesized by reaction of 2-(5-amino-1,3,4-thiadiazol-2-ylthio)acetohydrazide with different aromatic aldehydes or ketones.The structures of these compounds were characterized by IR,ESI-MS,1HNMR and 13CNMR. |
| |
| Keywords: | hydrazones 1 3 4-thiadiazol |
| 本文献已被 CNKI 等数据库收录！ |
|
