| 氮气鼓泡法制备L-丙交酯的新工艺 |
| |
| 引用本文： | 余家会,罗淑芳,俞磊,陈群. 氮气鼓泡法制备L-丙交酯的新工艺[J]. 广东化工, 2006, 33(6): 42-43,47 |
| |
| 作者姓名： | 余家会 罗淑芳 俞磊 陈群 |
| |
| 作者单位： | 华东师范大学,生物功能材料与器件研究所,上海,200062;华东师范大学,光谱学与波谱学教育部重点实验室,上海,200062 |
| |
| 基金项目： | 国家自然科学基金;上海市纳米科技专项基金 |
| |
| 摘 要： | 用氮气鼓泡法成功制得了L-丙交酯,此工艺路线中,氮气温度对丙交酯的生成至关重要,所得L-丙交酯粗品的纯度和产率比减压蒸馏所得L-丙交酯粗品的纯度和产率要高;用填料装置可完全吸收丙交酯;用活性炭对L-丙交酯粗品进行脱色比用沉淀法脱色效果好,收率较高。
|
| 关 键 词： | 氮气鼓泡法 L-丙交酯 制备 新工艺 |
| 收稿时间： | 2006-03-27 |
| 修稿时间： | 2006-03-27 |
Study on the New Technology for the Preparation of L-lactide with the Aid of Nitrogen Gas Bubble |
| |
| Yu Jiahui,Luo Shufang,Yu Lei,Chen Qun. Study on the New Technology for the Preparation of L-lactide with the Aid of Nitrogen Gas Bubble[J]. Guangdong Chemical Industry, 2006, 33(6): 42-43,47 |
| |
| Authors: | Yu Jiahui Luo Shufang Yu Lei Chen Qun |
| |
| Affiliation: | 1. Institute of Biofunctional Materials and Devices, East China Normal University, Shanghai 200062; 2. Key Laboratory of Optical and Magnetic Resonance Spectroscopy, Ministry of Education, East China Normal University, Shanghai 200062, China |
| |
| Abstract: | L-lactide was prepared with the aid of nitrogen gas bubble.The temperature of nitrogen is important for the preparation of L-lactide.The purity and yield of raw L-lactide prepared by nitrogen gas buble technology are higher than those of the raw L-lactide prepared by vacuum distillation.The capture of L-lactide is effective by using filling column and acetone as absorbent.The discoloring effectiveness of raw L-lactide with active carbon method is better than that of precipitation method. |
| |
| Keywords: | nitrogen-blowing L-lactide preparation new technology |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
