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| 有机硅改性丙烯酸酯乳液的合成和形态分析 | |
| 引用本文： | 严微,鲁琴,胡荣涛,杨婷婷,高庆,彭慧,程时远. 有机硅改性丙烯酸酯乳液的合成和形态分析[J]. 化学与生物工程, 2011, 28(8): 24-28. DOI: 10.3969/j.issn.1672-5425.2011.08.008 |
| 作者姓名： | 严微 鲁琴 胡荣涛 杨婷婷 高庆 彭慧 程时远 |
| 作者单位： | 1. 湖北大学材料科学与工程学院功能材料绿色制备与应用省部共建教育部重点实验室,湖北武汉,430062 2. 武汉华工图像技术开发有限公司,湖北武汉,430223 3. 武汉荟普化学新材料有限公司,湖北武汉,430030 |
| 基金项目： | 湖北省自然科学基金资助项目(2006ABA022); 湖北省教育厅科研项目(Q200610004) |
| 摘 要： | 以过硫酸铵(APS)为引发剂、十二烷基苯磺酸钠(SDBS)/辛基酚聚氧乙烯醚马来酸酯钠(OP-10)为复合乳化剂,利用含乙烯基的有机硅单体与丙烯酸酯类单体进行乳液聚合制备了甲基丙烯酸甲酯(MMA)/丙烯酸丁酯(BA)/有机硅(Si-1800)交联聚合物乳液.通过透射电子显微镜(TEM)观察乳胶粒形态的最佳染色方法为pH... |
| 关 键 词： | 丙烯酸酯 有机硅 乳胶粒 形态 |
Preparation and Morphological Analysis of Organic Silicone Modified Acrylate Emulsion |
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| YAN Wei,LU Qin,HU Rong-tao,YANG Ting-ting,GAO Qing,PENG Hui,CHENG Shi-yuan. Preparation and Morphological Analysis of Organic Silicone Modified Acrylate Emulsion[J]. Chemistry & Bioengineering, 2011, 28(8): 24-28. DOI: 10.3969/j.issn.1672-5425.2011.08.008 | |
| Authors: | YAN Wei LU Qin HU Rong-tao YANG Ting-ting GAO Qing PENG Hui CHENG Shi-yuan |
| Affiliation: | YAN Wei1,LU Qin2,HU Rong-tao3,YANG Ting-ting1,GAO Qing1,PENG Hui1,CHENG Shi-yuan1(1.Key Laboratory for the Green Preparation and Application of Functional Materials of Ministry of Education,School of Materials Science and Engineering,Hubei University,Wuhan 430062,China,2.Wuhan Huagong Image Technology & Development Co.Ltd.,Wuhan 430223,3.Wuhan Huipu New Chemical Materials Co.Ltd.,Wuhan 430030,China) |
| Abstract: | Methyl methactylate(MMA)/butyl acrylate(BA)/vinyl terminal polysiloxane(Si-1800) emulsion was prepared using ammonium persulfate(APS) as initiator,sodium dodylcyl benzene sulfonate(SDBS)/sodium(polyoxyethylated octyl phenol) maleate(OP-10) as compound emulsifier.The morphology of emulsion was observed by transmission electron microscropy(TEM).It had been found that the best staining method was by phosphotungstic acid(PTA) at pH value 2.0.Under above condition,the particle size was verified increasing with t... |
| Keywords: | acrylate silicone latex particle morphology |
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