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偏振同步荧光法与高效液相色谱联用在线同时检测芴及苊
引用本文:张勇,袁东星,吴兵,王新红,陈伟琪.偏振同步荧光法与高效液相色谱联用在线同时检测芴及苊[J].福建分析测试,1995(2).
作者姓名:张勇  袁东星  吴兵  王新红  陈伟琪
作者单位:厦门大学环境科学研究中心 厦门361005
摘    要:本文以高效液相色谱(HPLC)作为分离手段,以偏振同步荧光法为检测手段,实现了环境样品中芴、苊的在线同时测定。本方法对芴、苊检测限分别为0.039mg/L 和0.046mg/L。将该方法用于大气、海洋沉积物样品中芴、苊的在线同时测定、结果满意。

关 键 词:偏振同步荧光法  高效液相色谱  联用技术  芴、苊

Simultaneous Determination of Fluorene and Acenaphthene by On-Line Polarization Synchronous Fluorometry with HPLC
Zhang Yong Yuan Dongxing Wu Bing Wang Xinhong Chen Weiqi.Simultaneous Determination of Fluorene and Acenaphthene by On-Line Polarization Synchronous Fluorometry with HPLC[J].Fujian Anal Ysis & Testing,1995(2).
Authors:Zhang Yong Yuan Dongxing Wu Bing Wang Xinhong Chen Weiqi
Abstract:A novel analytical method has been established for on-line simultaneous determination of fluorene and acenaphthene by polarization synchronous fluorometry(PSF)hyphenated with HPLC.The detection limits were 0.039 and 0.046 mg L~(-1)for fluorene and acenaphthene,respec- tively.The proposed method has been successfully applied to simultaneous determination of fluo- rene and acenaphthene in environmental air and marine sediment samples.
Keywords:polarization synchronous fluorometry  HPLC  hyphenated technique  fluorene and acenaphthene
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