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反相流动注射分光光度法测定稀土铝合金中的稀土总量
引用本文:符连社 任英. 反相流动注射分光光度法测定稀土铝合金中的稀土总量[J]. 冶金分析, 1993, 13(6): 1-1
作者姓名:符连社 任英
作者单位:中国科学院长春应用化学研究所 长春130022(符连社),中国科学院长春应用化学研究所 长春130022(任英)
摘    要:本文以二溴—氯偶氮氯磷作显色剂,建立了反相流动注射分析测定稀土总量的方法.实验表明,本方法简便,快速,且钙、铁的允许量较手工法约提高一个数量级.方法用于稀土铝合金中的稀土总量的测定,结果满意.

关 键 词:二溴—氯偶氮氯膦  反相流动注射分析  铝合金  稀土

Determination of Total Rare Earths in Rare Earth Aluminium Alloys by Reverse Flow Injection Analysis
Fa Lianshe Ren Ying. Determination of Total Rare Earths in Rare Earth Aluminium Alloys by Reverse Flow Injection Analysis[J]. Metallurgical Analysis, 1993, 13(6): 1-1
Authors:Fa Lianshe Ren Ying
Abstract:In thispaper, a rapid and simple method for the determination of the total rare earths by reverse flow injection analysis is described. It based on the procedure of rare earths in 1.2 mol/L HC1 as carry stream and injecting DBC-CPA. The consumption of DBC-CPA is minimized and the permi-ting amounts of Ca and Fe are increased by about one order of magnitude as compared with that of manual method. The method has been used to determination of the total rare earths in rare earth aluminium alloys with satisfactory results.
Keywords:2- ( 4-Chloro-2-phosphonophenylazo ) -7- ( 2  6-dibromo-4-chloroplienylazo ) -1  8-dihydroxy -3   6-naphthalene disulfonic acid   Reverse flow injection analysis   Aluminium alloys   Rare earth
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