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超声-微波协同萃取紫参薯花青素工艺
引用本文:裴志胜,张海德,袁腊梅,辛晓晨,盛灵芝.超声-微波协同萃取紫参薯花青素工艺[J].食品科学,2012,33(2):78-83.
作者姓名:裴志胜  张海德  袁腊梅  辛晓晨  盛灵芝
作者单位:海南大学食品学院
基金项目:教育部高等学校博士学科点专项科研基金项目(20080565000);农业部热带作物种质资源保护专项(10RZZY-33);海南大学211工程建设创新人才培养项目
摘    要:以海南产紫参薯为原料,采用Box-Behnken中心组合试验设计优化紫参薯花青素的超声-微波协同萃取工艺。分别采用时间模式与恒温模式两种方法,在单因素试验基础上,以花青素提取率为响应值,采用三因素三水平的响应面分析法进行试验。结果表明:恒温模式时,在额定超声功率50W、料液比1:48(g/mL)、萃取时间283s、微波控制温度46℃工艺条件下,紫参薯提取率达79.38%,较时间模式下高10.63%,超声-微波协同萃取的总花青素质量浓度为48.42mg/L,即4.37mg/g。

关 键 词:紫参薯  花青素  超声-微波协同萃取(UMAE)  响应面优化  

Ultrasonic/Microwave-Assisted Extraction (UMAE) of Anthocyanins From Purple Yam
PEI Zhi-sheng,ZHANG Hai-de,YUAN La-mei,XIN Xiao-chen,SHENG Ling-zhi.Ultrasonic/Microwave-Assisted Extraction (UMAE) of Anthocyanins From Purple Yam[J].Food Science,2012,33(2):78-83.
Authors:PEI Zhi-sheng  ZHANG Hai-de  YUAN La-mei  XIN Xiao-chen  SHENG Ling-zhi
Affiliation:College of Food Science, Hainan University, Haikou 570228, China
Abstract:Purple yam planted in Hainan province(Dioscoreaceae,Dioscorea alata Linn) was used as the raw material to explore the optimal extraction process parameters of anthocyanins by ultrasonic/microwave assisted extraction technology.The optimal extraction process conditions were explored through Box-Benhnken central composite design.The results showed that the optimal extraction process conditions at the fixed temperature mode were ultrasonic power of 50 W,ultrasonic frequency of 40 kHz,material-liquid ratio of 1:48(g/mL),extraction time of 283 s and extraction temperature of 46 ℃.Under the optimal extraction conditions,the yield of anthocyanins was up to 79.38%,which revealed an enhancement by 10.63% compared with the fixed time mode.The total content of anthocyanins was 48.42 mg/L,namely 4.37 mg/g.
Keywords:purple yam  anthocyanins  ultrasonic/microwave-assisted extraction(UMAE)  response method
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