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某高硫磁铁精矿磁选—脱磁—复合活化反浮选脱硫试验
引用本文:廖军平,黄自力,崔军,叶子青,石家力. 某高硫磁铁精矿磁选—脱磁—复合活化反浮选脱硫试验[J]. 矿产保护与利用, 2019, 39(4): 125-130. DOI: 10.13779/j.cnki.issn1001-0076.2019.02.031
作者姓名:廖军平  黄自力  崔军  叶子青  石家力
作者单位:1.武汉科技大学 资源与环境工程学院,湖北 武汉 430081
摘    要:对TFe、S品位分别为55.61%、3.81%,主要硫化矿为磁黄铁矿和黄铁矿的某磁选铁精矿进行了系统的磁选—脱磁—复合活化反浮选脱硫试验研究。试验结果表明,该试样在磨矿细度-0.038 mm占88.32%条件下进行弱磁选,磁选精矿脱磁后,用硫酸调整矿浆pH值至5.5,以H2C2O4+CuSO4+Na2S为复合活化剂,高级黄药(烃基碳原子数为5~7,下同)+丁铵黑药为组合捕收剂,进行了一粗两扫三精反浮选全流程闭路试验,试验取得了铁精矿TFe品位66.71%、TFe回收率81.57%、S含量0.33%,副产品硫精矿S品位29.98%的良好指标。该研究较好地解决了矿山实际生产问题。 

关 键 词:铁精矿   脱硫   浮选   脱磁   磁铁矿   磁黄铁矿
收稿时间:2018-11-02

Desulfurization Experiment of a High Sulfur Iron Concentrate by Magnetic Separation-Demagnetization-Composite Activation Reverse Flotation
Affiliation:1.Wuhan University of Science and Technology, College of Resources and Environmental Engineering, Wuhan 430081, China2.Metallurgy and Mineral Resources Efficient Utilization and Building Block Hubei Key Laboratory, Wuhan 430081, China3.Qinghai Nanchuan Meige Metal Powder Exploiting Co. LTD., Geermu 730000, China
Abstract:Systematic magnetic separation-demagnetization-combined activation reverse flotation desulfurization experiments were carried out on a magnetic concentrate with the iron grade of 55.61% and the sulfur grade of 3.81% whose main sulfide ores are pyrrhotite and pyrite. The test results showed that the sample was subjected to a weak magnetic separation test under the condition of grinding fineness -0.038 mm accounting for 88.32%. After demagnetization of the magnetic separation concentrates, the closed-circuit test of the whole process of "one-stage roughing, two -stage scavenging, three-stage cleaning and reverse flotation" was carried out with the pulp pH of 5.5 adjusted by sulfuric acid, compound activator of H2C2O4+CuSO4+Na2S, and combined collector of the advanced xanthate (hydrocarbyl carbon number is 5-7) and the ammonium butyl aerofloat. The test finally obtained the iron concentrate grade of 66.71%, the iron recovery of81.57%, the sulfur content of 0.33%, and the by-product sulfur concentrate sulfur grade of 29.98%. The study better solved the actual production problems of the mine. 
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