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ICP-OES测定废水中总磷
引用本文:陈江,金新华,周均,吴惠英,吴杰. ICP-OES测定废水中总磷[J]. 工业水处理, 2011, 0(7): 83-85
作者姓名:陈江  金新华  周均  吴惠英  吴杰
作者单位:湖州市环境监测中心站,浙江湖州,313000
摘    要:为研究ICP-OES法测定废水中总磷,通过测定在不同射频功率、观测高度、载气流量和进样量条件下谱线的净强度,得到了灵敏度的变化规律.进行仪器参数优化后,测定样品.结果表明,检出限为0.05 mg/L,质控样相对误差为1.21%,相对标准偏差为0.96%(n=6),样品回收率为98.4%.该法试剂用量比常规的分光光度法少...

关 键 词:电感耦合等离子体  总磷  废水

Determination of total phosphorus in wastewater by ICP-OES
Chen Jiang,Jin Xinhua,Zhou Jun,Wu Huiying,Wu Jie. Determination of total phosphorus in wastewater by ICP-OES[J]. Industrial Water Treatment, 2011, 0(7): 83-85
Authors:Chen Jiang  Jin Xinhua  Zhou Jun  Wu Huiying  Wu Jie
Affiliation:Chen Jiang,Jin Xinhua,Zhou Jun,Wu Huiying,Wu Jie (Huzhou Environmental Monitoring Center,Huzhou 313000,China)
Abstract:For the purpos e of determining total phosphorus in wastewater by ICP-OES,the law of spectrum sensitivity change has been obtained by determining the spectrum intensity under different conditions,such as different RF power,observation height,carrier gas flow and injection volume.Samples are determined after optimizing the parameters of ICP.The results show that the detection limit is 0.05 mg/L,relative deviation of QC sample 1.21%,RSD 0.96%(n=6),and sample recovery rate about 98.4%.The dosage of reagent by ...
Keywords:inductively coupled plasma  total phosphorus  wastewater  
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