| 甘油三油酸酯的合成研究 |
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| 引用本文： | 张月成,户秋义,韩建萍,赵继全,韩双战,赵彦丽. 甘油三油酸酯的合成研究[J]. 精细石油化工, 2003, 0(6): 32-34 |
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| 作者姓名： | 张月成 户秋义 韩建萍 赵继全 韩双战 赵彦丽 |
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| 作者单位： | 1. 河北工业大学化工学院制药工程系,天津,300130
2. 维生药业石家庄有限公司,石家庄,050035 |
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| 摘 要： | 以对甲苯磺酸为催化剂合成了甘油三油酸酯 ,最佳工艺条件为催化剂用量为甘油质量的 6 .9% ,油酸过量 10 % ,反应时间 4 .5h ,反应温度 15 0～ 16 0℃时 ,产率达 92 .7%。建立了一套甘油三油酸酯的分离、分析检测方法。
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| 关 键 词： | 甘油三油酸酯 油酸 对甲苯磺酸 |
| 修稿时间： | 2003-01-22 |
STUDY ON SYNTHESIS OF GLYCEROL TRIOLEATE |
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| Zhang Yuecheng,Hu Qiuyi,Han Jianping,Zhao Jiquan,Han Shuangzhan and Zhao Yanli. STUDY ON SYNTHESIS OF GLYCEROL TRIOLEATE[J]. Speciality Petrochemicals, 2003, 0(6): 32-34 |
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| Authors: | Zhang Yuecheng Hu Qiuyi Han Jianping Zhao Jiquan Han Shuangzhan Zhao Yanli |
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| Affiliation: | Zhang Yuecheng1,Hu Qiuyi1,Han Jianping1,Zhao Jiquan1,Han Shuangzhan2 and Zhao Yanli2 |
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| Abstract: | The synthesis of glycerol trioleate from oleic acid and glycerol with toluene-p- sulfonic acid as catalyst was studied. The optimal conditions were obtained as follows: molar ratio of oleic acid to glycerol=1.1∶1, w(catalyst)=6.9% of glycerol, reaction temperature 150160 ℃, reaction time 4.5 h. The yield is 92.7%. The methods for separating and analyzing glycerol trioleate were given. |
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| Keywords: | glycerol trioleate oleic acid toluene-p- sulfonic acid |
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