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原子荧光光度法测定重整原料油中的微量砷
引用本文:安全建,曹敏.原子荧光光度法测定重整原料油中的微量砷[J].化学工业与工程技术,2008,29(6):49-51.
作者姓名:安全建  曹敏
作者单位:昆山市精细化工研究所有限公司,江苏,昆山,215337
摘    要:讨论了重整原料油试样消解的前处理过程,提出了消解时间短、反应温和、重现性好的前处理方法,采用氢化物原子荧光光度法测定砷含量,检出限为0.02ng/mL。实验结果表明,该方法在灵敏度、重现性、分析速度,尤其是批量分析等方面具有卓越的表现。

关 键 词:原子荧光光度法    重整原料油  酸消解

Determining the trace amount of arsenic in reforming material oil by atom fluorophotometry
An Quanjian,Cao Min.Determining the trace amount of arsenic in reforming material oil by atom fluorophotometry[J].Journal of Chemical Industry & Engineering,2008,29(6):49-51.
Authors:An Quanjian  Cao Min
Affiliation:(Kunshan Fine Chemical Research Institute Co. , Ltd. , Kunshan 215337, China)
Abstract:The pre-treatment process for counteraction of reforming material oil is discussed and the pre-treatment method with short counteraction time,temperate reaction condition and good repeatability is put forward.The content of arsenic is determined by atom fluorophotometry with detection limit of 0.02 ng/mL.The results show that the mentioned method has superiority in sensitivity,repeatability,analyse speed,especially in batch analyse.
Keywords:Atom fluorophotometry  Arsenic  Reforming material oil  Acid counteraction  
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