Synthesis and characterization of MFe2O4 (M = Mg,Mn, Ni) nanoparticles |
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| Affiliation: | 1. Materials Science Lab (1), Physics Department, Faculty of Science, Cairo University, Giza, Egypt;2. Department of Physics, Faculty of Science, Suez University, Suez, Egypt;3. TardigradeNano, Irvine, CA, 92604, USA;1. Faculty of Chemistry, Alexandru Ioan Cuza University, Bd. Carol I, nr. 11, Iasi 700506, Romania;2. Faculty of Physics, Alexandru Ioan Cuza University, Bd. Carol I, nr. 11, Iasi 700506, Romania;1. Department of Physics, Dhanalakshmi Srinivasan College of Engineering, Coimbatore 641105, India;2. Department of Physics, Government College of Technology, Coimbatore 641018, India;3. Department of Physics, Tamilnadu College of Engineering, Coimbatore 641659, India;1. Department of Physics, Nanotechnology Laboratory, Sri Ramakrishna Mission Vidyalaya College of Arts and Science, Coimbatore 641020, Tamil Nadu, India;2. Department of Physics, B.R. Ambedkar Bihar University, Muzaffarpur 842001, Bihar, India;1. V. I. Vernadskii Institute of General and Inorganic Chemistry, 32/34 Palladina Avenue, 03680 Kyiv 142, Ukraine;2. LUNAM, Institut des Molécules et Matériaux du Mans (IMMM UMR CNRS 6283), Université du Maine, 72085 Le Mans Cedex, France |
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| Abstract: | MFe2O4 nanoparticles were obtained in the presence of natural compounds as carboxymethylcellulose (CMC). The CMC polymer had a double function as a capping agent and as a protecting agent in the growth process of nanoparticles. The synthesized nanoparticles were characterized using thermal analysis (TG, DTA, DTG), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and a vibrating sample magnetometer (VSM). The XRD patterns indicate that all the samples were formed in single phase spinel structure. The results also show that the samples calcinated at 500 °C for 6 h have the best crystallinity and the calculated crystallite size was in the range of 6–13 nm. The thermal analysis and FTIR spectra indicate a core–shell structure of the MFe2O4 nanoparticles obtained. |
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