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Preparation of N-methylaniline capped mesoporous TiO2 spheres by simple wet chemical method
Affiliation:1. Department of Physics and Nanotechnology, SRM University, Kattankulathur, Kancheepuram 603203 (D.t.), Tamil Nadu, India;2. Research Institute of Electronics, Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu, Shizuoka 432-8011, Japan;1. Institute of Materials Science and Engineering, Ocean University of China, Qingdao 266100, Shandong Province, PR China;2. National Defense Key Disciplines Laboratory of Light Alloy Processing Science and Technology, Nanchang Hangkong University, Nanchang 330063, PR China;1. Key Laboratory of Biorheological Science and Technology (Chongqing University), Ministry of Education, and Key Lab of Visual Damage and Regeneration & Restoration of Chongqing, Chongqing, Bioengineering College, Chongqing University, Chongqing 400030, China;2. College of Pharmacy, Third Military Medical University, Chongqing 400038, China;1. School of Physics, Huazhong University Science and Technology, Wuhan 430074, China;2. School of Physics and Electronic Information, Huanggang Normal University, Huanggang 438000, China;3. Wu Han National Laboratory for Optoelectronics, Huazhong University Science and Technology, Wuhan 430074, China;4. National High Magnetic Field Center, Huazhong University Science and Technology, Wuhan 430074, China;1. Center for Materials Science and Nano Devices, Department of Physics, SRM University, Kattankulathur, Kancheepuram 603203, Tamil Nadu, India;2. Research Institute of Electronics, Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu, Shizuoka 432-8011, Japan;1. School of Materials Science and Engineering, Tsinghua University, Beijing 100084, China;2. Key Laboratory for Advanced Materials Processing Technology, Ministry of Education, Tsinghua University, Beijing 100084, China
Abstract:Pure anatase mesoporous TiO2 nanospheres were synthesized by simple wet chemical treatment and characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), ultraviolet–visible spectroscopy (UV–vis), Fourier transform infrared spectroscopy (FTIR) and powder X-ray diffraction (XRD). The results revealed that the surface morphology of the TiO2 spheres could be controlled by adjusting the concentration of N-methylaniline and that the average diameter of the TiO2 spheres was 600 nm. FTIR results confirmed the formation of N-methylaniline capped TiO2 nanospheres.
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