| 化橘红挥发油成分分析研究 |
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| 引用本文： | 李春,向能军,沈宏林,高茜,缪明明,赵逸云. 化橘红挥发油成分分析研究[J]. 精细化工中间体, 2009, 39(4): 65-67 |
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| 作者姓名： | 李春 向能军 沈宏林 高茜 缪明明 赵逸云 |
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| 作者单位： | 红塔烟草集团有限责任公司,技术中心,云南,玉溪,653100;云南大学,化学科学与工程学院,云南昆明,650021;红塔烟草集团有限责任公司,技术中心,云南,玉溪,653100;红塔烟草集团有限责任公司,技术中心,云南,玉溪,653100;昆明理工大学,化学工程学院,云南,昆明,650224;云南大学,化学科学与工程学院,云南昆明,650021 |
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| 摘 要： | 运用同时蒸馏萃取法提取中药化橘红挥发油成分，毛细管气相色谱-质谱联用技术对挥发油成分进行分离，峰面积归一化法定量分析，共分离出143种成分，鉴定出其中的61种成分，其含量占挥发油总量的94．5％。主要成分是：柠檬烯（75．8％）、棕榈酸（3．8％）等。
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| 关 键 词： | 同时蒸馏萃取 化橘红 挥发油 气相色谱一质谱联用 |
Studies on Chemical Constituents of Exocarpium Citri Grandis Volatile Oil |
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| LI Chun,XIANG Neng-jun,SHEN Hong-lin,GAO Qian,MIAO Ming-ming,ZHAO Yi-yun. Studies on Chemical Constituents of Exocarpium Citri Grandis Volatile Oil[J]. Fine Chemical Intermediates, 2009, 39(4): 65-67 |
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| Authors: | LI Chun XIANG Neng-jun SHEN Hong-lin GAO Qian MIAO Ming-ming ZHAO Yi-yun |
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| Affiliation: | LI Chun, XIANG Neng-jun, SHEN Hong-lin, GA O Qian, MIA O Ming-min , ZHA O Yi-yun ( 1. R＆D Center of Hong-Ta Tobacco Group Co.,Ltd., Yuxi 653100, China; 2. Department of Chemical Science and Engineering of Yunnan University, Kunming 650021, China; 3. School of Chemical Engineering of Kunming University of Science and Technology, Kunming 650224, China) |
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| Abstract: | Simultaneous distillation extraction (SDE) was coupled with gas chromatography-mass spectrometry (GC-MS)for separation of volatile oil from exocarpium citri grandis, a traditional Chinese medicine. The volatile oil compounds were quantified by the accuracy of area percent. It was separated into 143 components, among which 49 were identified, accounting to about 94.5% of the total volatile oil components. The main components are limonene (75.8%) and palmitic acid (3.8%). |
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| Keywords: | simultaneous distillation extraction ( SDE) exocarpium citri grandis volatile oil gas chromatography-mass spectrometry (GC-MS) |
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