| 3,4-乙撑二氧噻吩(EDOT)的新合成方法 |
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| 引用本文： | 钱先锋,李寒旭,丁立明,荚江霞. 3,4-乙撑二氧噻吩(EDOT)的新合成方法[J]. 化工新型材料, 2007, 35(2): 19-21 |
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| 作者姓名： | 钱先锋 李寒旭 丁立明 荚江霞 |
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| 作者单位： | 安徽理工大学化学工程系,淮南,232001;安徽理工大学化学工程系,淮南,232001;安徽理工大学化学工程系,淮南,232001;安徽理工大学化学工程系,淮南,232001 |
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| 摘 要： | 以氯乙酸为原料,通过酯化、Claisen缩合、O-烷基化和脱羧等反应合成出3,4-乙撑二氧噻吩,总产率为23.6%,运用FTIR、GC-MS对产品结构进行了表征,并对其反应机理进行了讨论.
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| 关 键 词： | PEDOT 3 4-乙撑二氧噻吩 导电材料 发光材料 |
| 修稿时间： | 2006-10-09 |
A new synthetic method of 3,4-ethylenedioxythiophene(EDOT) |
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| Qian Xianfeng,Li Hanxu,Ding Liming,Jia Jiangxia. A new synthetic method of 3,4-ethylenedioxythiophene(EDOT)[J]. New Chemical Materials, 2007, 35(2): 19-21 |
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| Authors: | Qian Xianfeng Li Hanxu Ding Liming Jia Jiangxia |
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| Abstract: | 3,4-ethylenedioxythiophene was synthesized from chloroacetic acid by esterification,Claisen condensation,O-alkylation and decarboxylation.The total yield of product was about 23.6%.The product was then characterized by FTIR and GC-MS,and the reaction mechanism was discussed. |
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| Keywords: | 3 4-ethylenedioxythiophene(PEDOT) conductive material luminescent material |
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