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Molten Salt Synthesis of Acicular Ba2NaNb5O15 Seed Crystals
Authors:Qing-Wei Huang  Jiong Xu  Li-Hui Zhu  Hui Gu   Pei-Ling Wang
Affiliation:The State Key Lab of High Performance Ceramics and Superfine Microstructures, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China; School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Abstract:Well-developed acicular Ba2NaNb5O15 (BNN) seed crystals have been successfully prepared by the reaction between BaCO3, Nb2O5 and molten NaCl salt. The effects of the calcination temperature, time, and weight ratio of the oxide mixture to salt on the morphology of BNN particles were investigated. Uniform acicular seeds with high aspect ratio could be achieved at 1200°C for 4 h with the salt-to-oxide mixture of 2:1.
Keywords:
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