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An improved process for the synthesis of titanium-rich titanium silicates (TS-1) under microwave irradiation |
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| Affiliation: | 1. School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255000, China;2. Department of Chemical Engineering, Tianjin Polytechnic University, Tianjin 300387, China;3. State Key Laboratory of Organic-Inorganic Composites, College of Chemical Engineering, Beijing University of Chemical Technology, Beijing 100029, PR China |
| Abstract: | Microwave irradiation is efficiently employed for the synthesis of crystalline titanium silicates with MFI structure and high titanium content (Si/Ti = 10) at extremely faster reaction rates. The physico-chemical properties and the phenol oxidation activity of these catalytic materials are similar to the titanium silicates synthesized by the conventional heating method. |
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