| 微波萃取/GC-MS测定纸质食品包装材料中双酚A |
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| 引用本文： | 蒋小良 陈梅 陈凯 等. 微波萃取/GC-MS测定纸质食品包装材料中双酚A[J]. 中华纸业, 2014, 0(6): 26-29 |
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| 作者姓名： | 蒋小良 陈梅 陈凯 等 |
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| 作者单位： | [1]江门出入境检验检疫局,广东江门529000 [2]中山大学物理科学和工程技术学院,广州510275 [3]东风日产乘用车公司,广州510800 |
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| 基金项目： | 广东省江门市科技计划项目（20120050104088）资助. |
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| 摘 要： | 以丙酮为萃取剂,建立了微波萃取/气相色谱-质谱法(GC-M S)测定纸质食品包装材料中双酚A含量的分析方法。考察了微波萃取温度与时间对萃取效果的影响,选择了最佳的微波萃取条件。结果表明:方法的检出限为0.05m g/kg,样品的加标回收率为84.2%~95.4%,相对标准偏差小于4.6%。该方法具有快速、方便、灵敏度高等优点,适合于纸质食品包装材料中双酚A含量的快速测定。
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| 关 键 词： | 微波萃取 双酚A 纸质食品包装材料 气相色谱-质谱法 |
Determination of bisphenol A in paper packaging material for foodstuffs by microwave extraction and GC-MS |
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| JIANG Xiao-liang,CHEN Mei,CHEN Kai,WANG Jie-quan. Determination of bisphenol A in paper packaging material for foodstuffs by microwave extraction and GC-MS[J]. China Pulp & Paper Industry, 2014, 0(6): 26-29 |
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| Authors: | JIANG Xiao-liang CHEN Mei CHEN Kai WANG Jie-quan |
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| Affiliation: | 1 (1.Jiangmen Entry-Exit Inspection and Quarantine Bureau, Jiangmen 529000; Guangdong China; 2.School of Physics and Engineering, Sun Yat-Sen University, Guangzhou 510275 China; 3.Dongfeng Nissian Passenger Vehicle Company, Guangzhou 510800, China) |
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| Abstract: | A method was developed for the determination of bisphenol A in paper packaging material for tbodstuffs by microwave extraction combined with a gas chromatography-mass spectrometry, acetone as extraction solvent, the effects of microwave extraction temperature and time were investigated and optimized. The results show that detection limit is 0.05 mg/kg, the range of 84.2%-95.4% with relative standard deviation（RSD） is below 4.6%. The method is rapid, simple, and accurate, can be used for the test ofpentachlorophenol in paper packaging material for foodstuffs. |
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| Keywords: | microwave extraction bisphenol A paper packaging material for foodstuffs gas chromatography-mass spectrometry |
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