| MCM-41沸石分子筛的微波合成与表征 |
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| 引用本文： | 赵杉林,张扬健,孙桂大,翟玉春.MCM-41沸石分子筛的微波合成与表征[J].石油化工,1999,28(3):139-140. |
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| 作者姓名： | 赵杉林 张扬健 孙桂大 翟玉春 |
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| 作者单位： | 1. 抚顺石油学院应化系,辽宁省抚顺,113001
2. 东北大学材料与冶金学院,沈阳,110006 |
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| 摘 要： | 以溴代十六烷基吡啶（ＣＰＢｒ）为模板剂，硅溶胶为硅源，用微波辐射的方法合成高结晶度的ＭＣＭ ４１中孔分子筛。探讨了微波晶化时间、微波反应釜压力等合成影响因素，确定了合适的配比范围及合成条件。利用ＸＲＤ、ＴＥＭ等方法对ＭＣＭ ４１中孔分子筛的物相和晶貌作了表征。
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| 关 键 词： | MCM-41分子筛 微波辐射 无机合成 表征 |
| 修稿时间： | 1998-06-03 |
The Characterization and Synthesis of Mesoporous Molecular Sieve MCM-41 by Microwave Radiation |
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| ZHAO Shan-lin,ZHANG Yang-jian,SUN Gui-da,ZHAI Yu-chun.The Characterization and Synthesis of Mesoporous Molecular Sieve MCM-41 by Microwave Radiation[J].Petrochemical Technology,1999,28(3):139-140. |
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| Authors: | ZHAO Shan-lin ZHANG Yang-jian SUN Gui-da ZHAI Yu-chun |
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| Abstract: | In this paper the synthesis of mesoporous molecular sieve MCM 41 with cetylpyridine bromide as templating agent by means of microwave radiation is reported for the first time.The synthesis conditions of crystallization time and pressure were investigated,the proper feedstock proportion and the technical parameters of preparing mesoporous molecular sieve MCM 41 by means of microwave radiation were evaluated.The structure of the crystal and property of the phase were studied by means of XRD and TEM techniques. |
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| Keywords: | mesoporous molecular sieves MCM 41 microwave radiation inorganic synthesis characterization |
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