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Effect of coagulation temperature on structures and properties of poly(p-phenylene benzobisoxazole) (DHPBO) fibers during dry-jet wet-spinning process
Authors:ZHANG Tao  JIN JunHong  HU DaYong  YANG ShengLin  LI Guang & JIANG JianMing State Key Laboratory for Modification of Chemical Fibers  Polymer Materials  College of Material Science  Engineering  Donghua University  Shanghai  China
Affiliation:ZHANG Tao,JIN JunHong,HU DaYong,YANG ShengLin,LI Guang & JIANG JianMing State Key Laboratory for Modification of Chemical Fibers , Polymer Materials,College of Material Science , Engineering,Donghua University,Shanghai 201620,China
Abstract:The effect of coagulation temperature on the morphology, microstructures and mechanical properties of dihydroxy poly(p-phenylene benzobisoxazole) (DHPBO) fibers was investigated during dry-jet wet- spinning process, in which the coagulation bath concentration and drawn ratio were kept as 10 wt% of PPA in water and 1.7, respectively. The structures and mechanical properties of the as-spun DHPBO fibers were characterized by FTIR, XRD, SEM, and single fiber tensile testing. The results indicated that in PPA/H2...
Keywords:DHPBO fibers  coagulation temperature  degree of crystallization  microstructures  mechanical properties  
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