| 沉淀法制备羟基磷灰石的工艺因素研究 |
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| 引用本文： | 张小立,张照军,刘英.沉淀法制备羟基磷灰石的工艺因素研究[J].中原工学院学报,2012,23(6):35-37,59. |
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| 作者姓名： | 张小立 张照军 刘英 |
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| 作者单位： | 中原工学院,郑州,450007 |
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| 基金项目： | 河南省科技厅国际合作项目，河南教育厅自然科学研究计划项目 |
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| 摘 要： | 研究了沉淀法制备羟基磷灰石（HAP）工艺中原料、陈化时间、pH值、Ca／P比及温度等因素对HAP纯度的影响．试验结果表明：反应溶液陈化时间要达到10～22h；当煅烧温度在900～1000℃之间时，可得到结晶程度较好的HAP粉体；反应时溶液的pH值应在10～12之间；制备HAP粉末时，Ca／P比为1．67时比1．00时所制的HAP粉末纯度高．
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| 关 键 词： | 羟基磷灰石 纯度 工艺因素 |
The Study on Technical Factor Influencing the Purity of HAP Prepared by Method of Precipitation |
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| ZHANG Xiao-li
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ZHANG Zhao-jun
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LIU Ying.The Study on Technical Factor Influencing the Purity of HAP Prepared by Method of Precipitation[J].Journal of Zhongyuan Institute of Technology,2012,23(6):35-37,59. |
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| Authors: | ZHANG Xiao-li ZHANG Zhao-jun LIU Ying |
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| Affiliation: | (Zhongyuan University of Technology,Zhengzhou 450007,China) |
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| Abstract: | The effect of raw material, aging time, pH value, the ratio of Ca/P and calcine temperature on purity of HAP were studied in this paper. The results showed that the aging time of solution should more than 10 hours. The calcine temperaure need to be at 90041 000℃; The PH value should be between 10~12; And when Ca/P is 1.67, the gained HAP will be more pure than Ca/P is 1.00. |
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| Keywords: | HAP purity technical factor |
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