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Targeted heat treatment of additively manufactured Ti-6Al-4V for controlled formation of Bi-lamellar microstructures
Authors:Cecilie V.Funch  Alessandro Palmas  Kinga Somlo  Emilie H.Valente  Xiaowei Cheng  Konstantinos Poulios  Matteo Villa  Marcel A.J.Somers  Thomas L.Christiansen
Abstract:Laser powder bed fusion (L-PBF) was utilized to produce specimens in Ti-6Al-4V,which were subjected to a bi-lamellar heat treatment,which produces microstructures consisting of primary α-lamellae and a fine secondary α-phase inside the inter-lamellar β-regions.The bi-lamellar microstructure was obtained as (i)a direct bi-lamellar heat treatment from the asbuilt condition or (ii) a bi-lamellar heat treatment preceded by a β-homogenization.For the bi-lamellar treatment with β-homogenization,cooling rates in the range 1-500 K/min were applied after homogenization in β-region followed by inter-critical annealing in the α + β region at various temperatures in the range 850-950 ℃.The microstructures were characterized using various microscopical techniques.Mechanical testing with Vickers hardness indentation and tensile testing was performed.The bi-lamellar microstructure was harder when compared to a soft fully lamellar microstructure,because of the presence of fine α-platelets inside the β-lamellae.Final low temperature ageing provided an additional hardness increase by precipitation hardening of the primary α-regions.The age hardened bi-lamellar microstructure shows a similar hardness as the very fine,as-built martensitic microstructure.The bi-lamellar microstructure has more favorable mechanical properties than the as-built condition,which has high strength,but poor ductility.After the bi-lamellar heat treatment,the elongation was improved by more than 250 %.Due to the very high strength of the as-built condition,loss of tensile strength is unavoidable,resulting in a reduction of tensile strength of~18 %.
Keywords:Additive manufacturing  Ti-6Al-4V  Targeted heat treatment  Bi-lamellar microstructures  Laser powder bed fusion
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