| ZSM-22分子筛的合成与表征 |
| |
| 引用本文： | 汪亚涛,徐军,韩丽,卫冬燕,陈宜俍.ZSM-22分子筛的合成与表征[J].天津化工,2011,25(5):21-23. |
| |
| 作者姓名： | 汪亚涛 徐军 韩丽 卫冬燕 陈宜俍 |
| |
| 作者单位： | 郑州大学化工与能源学院,河南 郑州,450001 |
| |
| 摘 要： | 以1,6-己二胺（DAH）为模版剂,在水热合成条件下考察了合成方法、添加晶源、不同硅源、晶化温度、硅铝比等因素对合成ZSM-22分子筛的影响。并采用XRD、SEM等方法对合成样品进行了表征。实验结果表明,在晶化温度为433 K、原料配比为90（SiO2）∶1（Al2O3）∶27（DAH）∶27（K2O）∶3 600（H2O）时,采用正硅酸乙酯为硅源,以动态合成法可合成结晶度良好的ZSM-22分子筛。
|
| 关 键 词： | ZSM-22分子筛 1 6-己二胺 合成 表征 |
Synthesis of and Characterization of ZSM-22 zeolite |
| |
| WANG Yatao,XU Jun,HAN Li,WEI Dong-yan,CHEN Yi-liang.Synthesis of and Characterization of ZSM-22 zeolite[J].Tianjin Chemical Industry,2011,25(5):21-23. |
| |
| Authors: | WANG Yatao XU Jun HAN Li WEI Dong-yan CHEN Yi-liang |
| |
| Affiliation: | WANG Yatao,XU Jun,HAN Li,WEI Dong-yan,CHEN Yi-liang(School of Chemical Engineering and Energy,Zhengzhou University,Zhengzhou Henan 450001,China) |
| |
| Abstract: | The ZSM-22 zeolite has been synthesized by means of the hydrothermal synthesis method using 1,6-diaminohexane as a template.The effect of synthesis conditions on ZSM-22 zeolite was studied.The synthesized sample were characterized by XRD and SEM.The synthesised ZSM-22 zeolite was highly crystalline and free of amorphous material under the following optimal dynamic synthesis conditions: temperature 433 K、90(SiO2)∶1(Al2O3)∶27(DAH)∶27(K2O)∶3 600(H2O),tetraethyl orthosilioate as the silica source. |
| |
| Keywords: | ZSM-22 zeolite 1 6-diaminohexane synthesis characterization |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
