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薄壳山核桃仁油甘油三酯成分分离鉴定
引用本文:许培源,袁博,左飞,李永荣,蒋继宏. 薄壳山核桃仁油甘油三酯成分分离鉴定[J]. 食品科学, 2014, 35(6): 159-163. DOI: 10.7506/spkx1002-6630-201406034
作者姓名:许培源  袁博  左飞  李永荣  蒋继宏
作者单位:江苏师范大学 江苏省药用植物生物生物技术重点实验室,江苏 徐州 221116
基金项目:江苏师范大学自然科研基金项目(12XLB04);江苏省高校青蓝工程优秀科技创新团队资助项目(药用微生物前期开发);江苏省研究生教育创新工程项目(CXLX11_0911)
摘    要:对薄壳山核桃仁油进行提取,利用制备型液相色谱-蒸发光散射-质谱联用技术分离和鉴定。分离得到7 个单体化合物,通过核磁与质谱数据比对,7 个单体化合物均为甘油三酯,分别为三亚油酸甘油酯、二亚油酸油酸甘油酯、棕榈酸二亚油酸甘油酯、亚油酸二油酸甘油酯、棕榈酸亚油酸油酸甘油酯、三油酸甘油酯、棕榈酸二油酸甘油酯。

关 键 词:薄壳山核桃油  分离鉴定  甘油三酯  
收稿时间:2013-06-02

Identification of Triacylglycerols from Pecan (Carya illinoensis) Oil
XU Pei-yuan,YUAN Bo,ZUO Fei,LI Yong-rong,JIANG Ji-hong. Identification of Triacylglycerols from Pecan (Carya illinoensis) Oil[J]. Food Science, 2014, 35(6): 159-163. DOI: 10.7506/spkx1002-6630-201406034
Authors:XU Pei-yuan  YUAN Bo  ZUO Fei  LI Yong-rong  JIANG Ji-hong
Affiliation:Key Laboratory of Biotechnology for Medicinal Plants of Jiangsu Province, Jiangsu Normal University, Xuzhou 221116, China
Abstract:Seven monomeric compounds from pecan (Carya illinoensis) oil were separated and identified by preparative
high performance liquid chromatography with evaporative light scattering detection combined with mass spectrometry
(HPLC-ELSD-MS). All these compounds were confirmed as triglycerides by comparison of their NMR and MS data with
those of authentic standards or literature data, namely trilinolein, dilinolein, 1,2-dilinoleoyl-3-palmitoyl-rac-glycerol,
dioleoylglycerol, 1-palmitin-2-olein-3-linolein, glycerol trioleate, dioleoyl 2-palmitoyl triglyceride, respectively.
Keywords:Carya illinoensis oil  separation and identification  triacylglycerols  
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