| 铝合金中磷的测定 |
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| 引用本文： | 李建舫.铝合金中磷的测定[J].兵器材料科学与工程,2005,28(5):48-50. |
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| 作者姓名： | 李建舫 |
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| 作者单位： | 中国兵器科学研究院,宁波分院,浙江,宁波,315103 |
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| 摘 要： | 采用盐酸溶解铝合金试样,高氯酸冒烟将磷氧化成正磷酸在0.42mol·L盐酸介质中,用抗坏血酸还原为铋磷钼蓝进行光度测定。经过条件试验,基体不干扰测定。对合成试样进行测定,回收率在91%-105%之间。该方法操作简便,结果准确可靠。
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| 关 键 词： | 铝合金 磷 分光光度计 |
| 文章编号： | 1004-244X（2005）05-0048-02 |
| 收稿时间： | 2005-01-11 |
| 修稿时间： | 2005-07-15 |
Determination of phosphorous in aluminium alloy |
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| LI Jian-fang.Determination of phosphorous in aluminium alloy[J].Ordnance Material Science and Engineering,2005,28(5):48-50. |
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| Authors: | LI Jian-fang |
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| Abstract: | Thesample was dissolved by HCL Phosphorus was oxidized to phosphorie acid, which was then reduced to molybdobismuthy phosphoric acid in mediator of 0.42 mol·L-1 HCl by ascorbic acid and then phosphorus was determinated by spectrophotometric method. The associated sample was also determinated. Recovery rate is at 91%-105%. The method is easy to operate and has high accuracy and precision. |
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| Keywords: | aluminium alloy phosphorus speetrophotometry method |
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