Solubility of N-chloro succinimide in different pure solvents in the temperature range from 278.15 K to 333.15K |
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Authors: | Jing Zhu Fei Shen Yong-Hong Hu Xin-min Jiang Dong-yun Li |
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Affiliation: | 2. School of Pharmaceutical Sciences, Nanjing University of Technology, Nanjing, 211816, China 1. Jiangsu Engineering Technology Research Center of Polypeptide Pharmaceutical, Nanjing, 210009, China
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Abstract: | Solubility data were measured for N-chloro succinimide in pure n-butanol, ethyl acetate, acetone, isopropanol, tetrahydrofuran, acetonitrile and acetic anhydride at the temperature range between 278.15 K and 333.15 K under atmospheric pressure by gravimetric method. The solubility of N-chloro succinimide in those selected solvents increased with increasing temperature. The solubility data were correlated with the modified Apelblat equation and the van??t Hoff equation to obtain the model parameters. The experimental results could be useful for optimizing the process of purification of N-chloro succinimide in industry. Isopropanol could be the excellent solvent in the crystallization of N-chloro succinimide. |
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