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超临界CO2萃取山苍子核仁油的工艺研究
引用本文:陈铁壁,袁先友,张敏.超临界CO2萃取山苍子核仁油的工艺研究[J].林产化工通讯,2009(1):5-8.
作者姓名:陈铁壁  袁先友  张敏
作者单位:湖南科技学院化学与生命工程学院,湖南永州425100
基金项目:湖南省“十一五”重点学科建设项目(2006-180);永州市科技计划项目(2006)
摘    要:研究了用超临界CO2流体萃取山苍子核仁油的萃取工艺,探讨了各种影响因素对山苍子核仁油萃取率的影响,通过正交试验确定了超临界萃取的最佳工艺为:萃取温度45℃、萃取压力25 MPa、CO2流量220 L/h、萃取时间80 min。在此条件下,山苍子核仁油萃取率84.5%。研究证明了加入溶剂和剥壳均可提高山苍子核仁油的萃取率。

关 键 词:山苍子核仁油  超临界CO2萃取

Study on Extraction Technology of Litsea cubeba Kernel Oil by Supercritical Carbon Dioxide
CHEN Tie-bi,YUAN Xian-you,ZHANG Min.Study on Extraction Technology of Litsea cubeba Kernel Oil by Supercritical Carbon Dioxide[J].Journal of Chemical Industry of Forest Products,2009(1):5-8.
Authors:CHEN Tie-bi  YUAN Xian-you  ZHANG Min
Affiliation:(Chemistry and bioengineering academy,Hunan University of Science and Engineering, Yongzhou 425100, China)
Abstract:An isolation technology of Litsea cubeba kernel oil in a dynamic supercritical fluid extraction system was described. Factors influencing extraction yield were discussed. By orthogonal test, the optimum technological conditions were:extraction temperature 45 ℃, pressure 25 MPa, flow rate of carbon dioxide 220 L/h and extraction time 80 min. The yield of extraction was 84.5 %. It is proved that adding the solvent and finding shell may improve extraction rates of Litsea cubeba kernel oil.
Keywords:Litsea cubeba kernel oil  SCDE( supercritical carbon dioxide extraction)
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