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Morphology of CuO through precipitation process under 2.45 GHz microwave irradiation
Authors:Ryoji Katoh  Masakuni OzawaYoshitaka Ino  Akira Kagohashi
Affiliation:a Ceramics Research Laboratory, Nagoya Institute of Technology, Tajimi, Gifu 507-0071, Japan
b Takasago Industry Co., Ltd., Toki, Gifu 509-5401, Japan
Abstract:The morphology of CuO powders formed by a homogeneous precipitation process from aqueous copper precursor complex was investigated. The effect of 2.45 GHz microwave irradiation appeared in the characteristic morphology of the CuO microcrystal with comparison of an ordinal synthesis process. The crystallographic orientation of CuO microcrystals in the particle was examined by HRTEM. Using microwave irradiation, it was demonstrated that the morphology of the particles was kept through the decomposition of the precursor. Also the rapid transformation of a precursor to CuO in aqueous solution under microwave irradiation condition was discussed.
Keywords:Microwave processing  Powders-chemical preparation  Electron microscopy  Microstructure-final  Structural applications
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