| 2,3,5,6-四氟苯甲腈的合成 |
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| 引用本文： | 何光文,陈宏博,戎娟.2,3,5,6-四氟苯甲腈的合成[J].辽东学院学报(自然科学版),2008,15(2). |
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| 作者姓名： | 何光文 陈宏博 戎娟 |
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| 作者单位： | 大连理工大学化学化工学院化学系,辽宁,大连,116012 |
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| 摘 要： | 以2,3,5,6-四氟苯甲酸为原料,经过酰氯制得酰胺后,再经脱水制得2,3,5,6-四氟苯甲腈,总收率61.8%,产品含量98%,这是一条最有望工业化的合成路线。
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| 关 键 词： | 2 3 5 6-四氟苯甲酸 2 3 5 6-四氟苯甲腈 脱水 |
Sythesis of 2,3,5,6-tetrafluoroaniline |
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| HE Guang-wen,CHEN Hong-Bo,RONG Juan.Sythesis of 2,3,5,6-tetrafluoroaniline[J].Journal of Liaodong University：Natural Sciences,2008,15(2). |
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| Authors: | HE Guang-wen CHEN Hong-Bo RONG Juan |
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| Abstract: | Using 2,3,5,6-tetrafluorobenzoic acid as raw material,2,3,5,6-tetrafluorobenzonitrile was prepared by a serial reactions including acyl chlorination,amidation and dehydration.The total yield was 61.8 % and product content 98 %.This is a hopeful way to industrially synthesize 2,3,5,6-tetrafluorobenzonitrile. |
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| Keywords: | 2 3 5 6-tetrafluorobenzoic acid 2 3 5 6tetrafluorobenzonitrile dehydration |
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