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Synthesis and characterization of poly(keto-amines). 1. Self polycondensation of 4-aminophenacyl chloride
Authors:Raman N. Patel  Shanti R. Patel
Affiliation:Institute of Chemistry, Nicholas Copernicus University, 87-100, Toruń, Poland
Abstract:Novel poly(keto-amines), designated as poly(4-iminophenacyls) are prepared by self polycondensation of 4-aminophenacyl chloride under different experimental conditions. These polymers are insoluble in common solvents. The number average molecular weights of the polymer samples have been estimated by conductometric titration of a suspension of the polymer sample in formic acid against a standard perchloric acid. The polymer samples have been characterized by a comparative study of their IR spectra with those of the probable model compounds and by differential thermogravimetric analysis.
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