层状钴酸锶铋热电陶瓷制备的研究 |
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引用本文: | 李国晶,张明强,赵淑金,杨涵崧,王涛.层状钴酸锶铋热电陶瓷制备的研究[J].佳木斯工学院学报,2010(2):251-253. |
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作者姓名: | 李国晶 张明强 赵淑金 杨涵崧 王涛 |
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作者单位: | [1]佳木斯大学材料科学与工程学院,黑龙江佳木斯154007 [2]佳木斯大学印刷厂,黑龙江佳木斯154007 |
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基金项目: | 佳木斯大学科研项目(L2009-095)资助;校重点项目(Lz2009-012)资助. |
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摘 要: | 实验采用熔融法和普通固相烧结法制备镧掺杂钴酸锶铋陶瓷.利用TG—DSC,XRD和SEM等测试方法对陶瓷样品热分解过程、物相和形貌进行表征.实验结果表明:熔融法能够更好的制备出致密度高、晶粒发育完整、片层结构明显、晶粒具有一定取向的陶瓷样品.制备工艺对样品的显微结构和热电性能有重要影响.
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关 键 词: | 熔融法 普通固相烧结法 Bi0.5-xLaxSr0.5Co Oy 陶瓷 |
Study on Preparation of Layered Structure Bi0.5-xLaxSr0.5Co Oy Thermoelectric Ceramics |
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Authors: | LI Guo-jing ZHANG Ming-qiang ZHAO Shu-jin YANG Han-song WANG Tao |
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Affiliation: | 1. College of Materials Science and Engineering, Jiamusi University, Jiamusi 154007, China; 2. Printing House, Jiamusi University, Jiamusi 154007, China) |
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Abstract: | Samples of Bi0.5-xLaxSr0.5Co Oy ceramics havC been prepared by melting method and common solid--state reaction. The pyrolytic decomposition mechanism, phase composition and microstructure of the samples are investigated by TG/DSC, XRD and SEM. The results show that ceramics samples fabricated by melting method are of high relative density, perfect fine--grains, plate--shaped structure and orientated grains. The preparation technologies can influence the microstructure and thermoelectric properties of ceramics samples greatly. |
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Keywords: | melting method common solid--state reaction method Bi0 5-xLaxSr0.5Co Oy ceramics |
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