基质辅助激光解析电离-飞行时间质谱在高分子聚合物研究应用中的样品制备方法 |
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引用本文: | 向弘,朱斌,徐昕荣,胡朝辉,杨豪. 基质辅助激光解析电离-飞行时间质谱在高分子聚合物研究应用中的样品制备方法[J]. 广东化工, 2009, 36(8): 85-86,117,118 |
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作者姓名: | 向弘 朱斌 徐昕荣 胡朝辉 杨豪 |
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作者单位: | 华南理工大学,分析测试中心,广东,广州,510640;邯郸市疾病预防控制中心,河北,邯郸,056002;广东工业大学大学,环境科学与工程学院,广东,广州,510006 |
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摘 要: | 在基质辅助激光解析电离.飞行时间质谱(Matxa ssisted laser desorption/ionization time—of-flight massspectrum,MALDI—TOF—MS)研究高分子聚合物的过程中,样品的制备方法对获得准确的质谱图非常关键,样品制备必须选择合适的溶剂、基质和阳离子化试剂。文章就近年来MALDI-TOF—MS在高分子聚合物研究中的有关样品制备方法的发展进行综述。
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关 键 词: | 基质辅助激光解析电离-飞行时间质谱 高分子聚合物 样品制备 |
Development of Sample Preparation Methods in the Study of Polymers Using Matrix Assisted Laser Desorption/ionization Time-of-Flight Mass Spectrum |
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Affiliation: | Xiang Hong, Zhu Bin, Xu Xingrong, Hu Chaohui ( Analytical and Testing Center, South China University of Technology, Guangzhou 510640; 2. Handan Municipal Center for Disease Prevention and Control, Handan 056002, China) |
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Abstract: | During the study of polymers by matrix assisted laser desorption/ionization time-of-flight mass spectrum (MALDI-TOF-MS), the sample preparation method is important to obtain the desired critical mass spectrometry. The polymer solvent, the mixture and the cationic reagents must be matched with the sample type. In this paper, the developments of sample preparation methods of MALDI-TOF-MS in the study of polymers on were reviewed. |
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Keywords: | matrix assisted laser desorption/ionization time-of flight mass spectrum polymer sample preparation |
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