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磁铁矿铁磁性能解析及应用
引用本文:王丽杰,丁欣,褚鸿锐,杨羽翼.磁铁矿铁磁性能解析及应用[J].材料科学与工艺,2016,24(6):90-96.
作者姓名:王丽杰  丁欣  褚鸿锐  杨羽翼
作者单位:测控技术与仪器黑龙江省高校重点实验室(哈尔滨理工大学) ,哈尔滨150080;哈尔滨理工大学 测控技术与通信工程学院,哈尔滨150080
基金项目:国家自然科学基金(61179023).
摘    要:探讨磁铁矿物理化学特性,研究单线圈阻抗检测方法,用其实现铁矿选矿工艺过程中全铁品位指标的在线自动监测.采用X射线衍射分析方法和电感耦合等离子体质谱方法表征磁铁矿原矿及铁精粉矿样的物相组成及化学成分.利用振动样品磁强计测试矿样的磁化强度、矫顽力、比磁化系数等磁学性能指标,解析磁铁矿的强磁性能,应用其铁磁特性探讨交流激磁、矩型电感线圈、磁铁矿铁芯等条件下全铁品位指标的电磁感应测量方法及测试机理.设计信息采集装置、信号调理电路以及PIC单片机控制系统,给出温湿度测试方法及温度补偿方案.实验测试结果表明:应用磁铁矿铁磁特性进行全铁品位指标电磁效应在线监测具备可行性,铁精粉干粉实验测试误差低于±0.5%,测量标准差为0.19%.

关 键 词:材料结构及物理性质  磁铁矿  X射线衍射分析  电感耦合等离子体质谱  铁磁性  全铁品位  电感线圈
收稿时间:2016/5/18 0:00:00

Analysis and exploitation ferromagnetic properties of magnetite
WANG Lijie,DING Xin,CHU Hongrui and YANG Yuyi.Analysis and exploitation ferromagnetic properties of magnetite[J].Materials Science and Technology,2016,24(6):90-96.
Authors:WANG Lijie  DING Xin  CHU Hongrui and YANG Yuyi
Affiliation:The Higher Educational Key Laboratory for Measuring & Control Technology and Instrumentations of Heilongjiang Province Harbin University of Science and Technology ,Harbin 150080, China ;School of Measurement-Control Technology and Communications Engineering, Harbin University of Science and Technology, Harbin 150080, China,The Higher Educational Key Laboratory for Measuring & Control Technology and Instrumentations of Heilongjiang Province Harbin University of Science and Technology ,Harbin 150080, China ;School of Measurement-Control Technology and Communications Engineering, Harbin University of Science and Technology, Harbin 150080, China,The Higher Educational Key Laboratory for Measuring & Control Technology and Instrumentations of Heilongjiang Province Harbin University of Science and Technology ,Harbin 150080, China ;School of Measurement-Control Technology and Communications Engineering, Harbin University of Science and Technology, Harbin 150080, China and The Higher Educational Key Laboratory for Measuring & Control Technology and Instrumentations of Heilongjiang Province Harbin University of Science and Technology ,Harbin 150080, China ;School of Measurement-Control Technology and Communications Engineering, Harbin University of Science and Technology, Harbin 150080, China
Abstract:The physical and chemical properties of magnetite were examined, which formed the basis for the development of an impedance detection method of single coil for online automatic monitoring for total iron (TFe) grade of iron ore during mining process. By using X-ray diffraction analysis method and inductively coupled plasma mass spectrometry (ICP-MS) method, phase composition and chemical composition of raw magnetite samples and fine iron powder samples were characterized. Furthermore, magnetic property indexes such as magnetization intensity, coercivity, and massic magnetic susceptibility, were detected by using vibrating sample magnetometer, and ferromagnetic properties of the magnetite were analyzed. According to the ferromagnetism, the principle behind the electromagnetic induction detection method for TFe grade under the condition of AC excitation and rectangle inductance coil with magnetite iron core was researched. Moreover, data acquisition devices were developed, signal processing circuits were designed, and PIC single-chip microcomputer control system was debugged. At the same time, temperature and moisture measuring methods were investigated, and temperature compensation scheme was given. The experiment results show that TFe grade test error is below ±0.5%, with a standard deviation of about 0.19%, and it is feasible and practicable for the on-line monitoring of electromagnetic effect of TFe grade by using ferromagnetic properties of magnetite.
Keywords:material structure and physical properties  magnetite  X-ray diffraction analysis  inductively coupled plasma mass spectrometry (ICP-MS)  ferromagnetism  total iron grade  inductance coil
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