| 滁菊亚临界净油挥发性和半挥发性成分分析及卷烟加香效果 |
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| 引用本文： | 王甜,赵明月,何保江,霍现宽,徐秀娟,徐志强,卓浩廉,谢金栋,马宇平,胡军. 滁菊亚临界净油挥发性和半挥发性成分分析及卷烟加香效果[J]. 烟草科技, 2015, 48(7): 46-52. DOI: 10.16135/j.issn1002-0861.20150709 |
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| 作者姓名： | 王甜 赵明月 何保江 霍现宽 徐秀娟 徐志强 卓浩廉 谢金栋 马宇平 胡军 |
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| 作者单位： | 1.1. 中国烟草总公司郑州烟草研究院, 郑州高新技术产业开发区枫杨街2号 450001;2.2. 安徽中烟工业有限责任公司技术研发中心, 合肥市蜀山区天达路9号 230088;3.3. 广东中烟工业有限责任公司技术研发中心, 广州市荔湾区东沙环翠南路88号 510385;4.4. 福建中烟工业有限责任公司技术研发中心, 福建省厦门市海沧区新阳工业区新阳路1号 361022;5.5. 河南中烟工业有限责任公司技术研发中心, 郑州市陇海东路72号 450000 |
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| 基金项目： | 中国烟草总公司科技重大专项项目"滁菊显效组分的靶向分离及其在焦甜香品类中的应用研究"[110201301030(BR-05)];中国烟草总公司郑州烟草研究院科技项目"亚临界萃取技术在烟用天然香料提取中的应用"(422013CZ0610) |
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| 摘 要： | 以滁菊为原料,利用亚临界技术提取滁菊净油;分别采用丁烷、丁烷+乙醇(夹带剂)、二甲醚和二甲醚+水(夹带剂)4种溶剂进行提取,采用GC/MS法对比分析了不同溶剂提取净油挥发性和半挥发性成分的差异,并用所得净油分别进行卷烟加香评吸实验。结果表明:①4种溶剂提取的净油中共鉴定出48种化学成分,包括21种烯类、10种醇类、7种酮类、3种酯类、2种羧酸及其他成分。②4种净油中对应成分质量分数的差异较大。随提取溶剂极性的增大,挥发性和半挥发性成分的质量分数逐渐降低。③以二甲醚为提取溶剂时,所得净油能较好地改善口感,卷烟烟气香气质和香气量改善,杂气降低,刺激性减小。
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| 关 键 词： | 亚临界提取 滁菊 净油 气相色谱-质谱法(GC/MS) 卷烟加香 |
| 收稿时间： | 2014-09-26 |
Analysis of Volatile and Semi-volatile Components in Chrysanthemum morifolium Ramat Absolute Prepared by Subcritical Extraction Technology and its Application to Cigarette Flavoring |
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| WANG Tian,ZHAO Mingyue,HE Baojiang,HUO Xiankuan,XU Xiujuan,XU Zhiqiang,ZHUO Haolian,XIE Jindong,MA Yuping,HU Jun. Analysis of Volatile and Semi-volatile Components in Chrysanthemum morifolium Ramat Absolute Prepared by Subcritical Extraction Technology and its Application to Cigarette Flavoring[J]. Tobacco Science & Technology, 2015, 48(7): 46-52. DOI: 10.16135/j.issn1002-0861.20150709 |
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| Authors: | WANG Tian ZHAO Mingyue HE Baojiang HUO Xiankuan XU Xiujuan XU Zhiqiang ZHUO Haolian XIE Jindong MA Yuping HU Jun |
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| Affiliation: | 1.1. Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China;2.2. R & D Center, China Tobacco Anhui Industrial Co., Ltd., Hefei 230088, China;3.3. R & D Center, China Tobacco Guangdong Industrial Co., Ltd., Guangzhou 510385, China;4.4. R & D Center, China Tobacco Fujian Industrial Co., Ltd., Xiamen 361022, Fujian, China;5.5. R & D Center, China Tobacco Henan Industrial Co., Ltd., Zhengzhou 450000, China |
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| Abstract: | The absolutes of Chrysanthemum morifolium Ramat were extracted by subcritical technology with 4 solvents,including butane,butane and ethanol(as entrainer),dimethyl ether,dimethyl ether and water(as entrainer) separately.The volatile and semi-volatile components in the obtained absolutes were analyzed by GC/MS method.The 4 absolutes were added into cigarettes as flavors,and sensory evaluation was conducted.The results showed that:1)48 chemical components identified in the 4 absolutes included 21 olefins,10 alcohols,7 ketones,3 esters,2 carboxylic acids among others.2) The contents of components in the absolutes differed significantly,and decreased with the increase of the polarity of extraction solvent.3) The absolute extracted with dimethyl ether effectively improved the taste,enhanced aroma quality,aroma quantity and reduced the offensive odor,irritancy of cigarette smoke. |
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