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正交试验法确定低品位钾矿溶解的最佳条件
引用本文:姜 虹,王 晓,王爱丽.正交试验法确定低品位钾矿溶解的最佳条件[J].无机盐工业,2015,47(5):24.
作者姓名:姜 虹  王 晓  王爱丽
作者单位:青海大学化工学院,青海西宁 810016
摘    要:以青海马海盐矿为原料,采用正交试验法研究盐矿中K+、Na+的溶解规律。一定的溶矿时间后,用正交试验法研究了液固比、溶剂中氯化钠的含量及溶剂中氯化镁的含量这3个素对矿液中K+、Na+含量的影响,并对正交试验的结果做了SPSS分析。3因素对试验结果中K+、Na+含量影响的主次顺序:液固比>溶剂中氯化钠的含量>溶剂中氯化镁的含量。实验确定了溶矿的最佳条件:液固比为1∶0.5、溶剂中氯化钠的质量分数为其饱和度的50%、溶剂中氯化镁的质量分数为3%。最佳条件下KCl的质量分数大于1.2%,符合要求,且NaCl的溶解量很小,达到不使盐矿骨架坍塌的要求。

关 键 词:盐矿溶解  正交试验  SPSS  

Optimum conditions for dissolution of low grade potassium ore confirmed by orthogonal test
JIANG Hong,WANG Xiao,WANG Ai-Li.Optimum conditions for dissolution of low grade potassium ore confirmed by orthogonal test[J].Inorganic Chemicals Industry,2015,47(5):24.
Authors:JIANG Hong  WANG Xiao  WANG Ai-Li
Affiliation:School of Chemical Engineering,Qinghai University,Xining 810016,China
Abstract:With Mohair salt mine,in Qinghai Province as raw material,the dissolution laws of K+ and Na+ from the salt mine were studied by orthogonal experiments.After a certain time of dissolution mine,the influences of three factors,ratio of liquid to solid,sodium chloride content in the solvent,and magnesium chloride content in the solvent on the contents of  K+ and Na+ in the liquid were investigated by orthogonal test method and the experiment results were analyzed with SPSS. The test results showed the influencing order for K+ and Na+ contents was:liquid to solid ratio>sodium chloride in solvent>magnesium chloride in solvent.The optimum conditions for the mineral dissolution were confirmed as follows:liquid-solid ratio was 1∶0.5,the content of sodium chloride was 50%(mass fraction,and same below) of its saturation in the solvent,the content of magnesium chloride was 3% in the solvent.Under optimal conditions the content of KCl was more than 1.2% which met the relevant requirements,and the small amount of dissolved NaCl also reached the requirements that the salt mine skeleton will not collapse.
Keywords:potassium mineral dissolving  orthogonal test  SPSS  
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