新型吸附材料制备及处理含DMAC废水试验研究* |
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作者单位: | 1.中国矿业大学环境与测绘工程学院,江苏徐州 221116;2.淮海工学院化学工程学院 |
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摘 要: | 合成了主要成分为粉煤灰和活性炭的新型吸附材料,并通过单因素试验考察了吸附材料处理含DMAC(N, N-二甲基乙酰胺)废水的效果。吸附材料最佳制备条件:粉煤灰与活性炭质量比为3∶1,硅酸钠加入量为25%(硅酸钠占粉煤灰、活性炭、硅酸钠总质量的质量分数),煅烧温度为800 ℃。吸附材料处理含N, N-二甲基乙酰胺废水最佳条件:pH为3,吸附剂投加量为25 g/L,吸附时间为40 min,吸附温度为30 ℃,在此条件下CODCr去除率为75.92 %。
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关 键 词: | 粉煤灰 硅酸钠 N N-二甲基乙酰胺 活性炭 |
Preparation of a new type of adsorption material to treat DMAC contained wastewater |
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Affiliation: | 1.School of Environment Science and Spatial Informatics,China University of Mining & Technology,Xuzhou 221116,China;
2.School of Chemical Engineering; Huaihai Institute of Technology |
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Abstract: | The adsorption performance of a new type of adsorption material based on the fly ash and activated carbon as main contents was researched.The effect of it treating DMAC(N,N-dimethyl acetamide) contained wastewater was investigated by the single factor experiment.The optimum preparation conditions:the mass ratio of fly ash to activated carbon was 3∶1,sodium silicate dosage was 25%(mass fraction of sodium silicate accounts for total mass of fly ash,activated carbon,and sodium silicate), and the calcining temperature was 800 ℃.The optimum conditions of the new material treating the DMAC wastewater were: pH was 3,adsorbent dosage was 25 g/L,absorbing time was 40 min,and absorbing temperature was 30 ℃.The removal rate of CODCr reached 75.92% under the best conditions. |
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Keywords: | fly ash sodium silicate DMAC activated carbon |
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