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双环戊二烯马来酸单酯的合成与表征
引用本文:俎喜红,胡剑青,涂伟萍. 双环戊二烯马来酸单酯的合成与表征[J]. 化学试剂, 2007, 29(11): 667-669
作者姓名:俎喜红  胡剑青  涂伟萍
作者单位:华南理工大学,化工与能源学院,广东,广州,510640;华南理工大学,化工与能源学院,广东,广州,510640;华南理工大学,化工与能源学院,广东,广州,510640
摘    要:通过顺丁烯二酸酐水解并与双环戊二烯发生酸催化加成反应,合成了标题化合物(DHCM),收率达90%,产品中w(DHCM)>85%。通过元素分析、红外光谱和GC-MS等对其结构进行了表征。

关 键 词:双环戊二烯马来酸单酯  合成  双环戊二烯  顺丁烯二酸酐
文章编号:0258-3283(2007)11-0667-03
修稿时间:2007-05-24

Synthesis and characterization of dicyclopentadiene monomaleate
ZU Xi-hong,HU Jian-qing,TU Wei-ping. Synthesis and characterization of dicyclopentadiene monomaleate[J]. Chemical Reagents, 2007, 29(11): 667-669
Authors:ZU Xi-hong  HU Jian-qing  TU Wei-ping
Affiliation:Institute of Chemical and Energy Engineering,South China University of Technology,Guangzhou 510640,China
Abstract:Dicyclopentadiene monomaleate(DHCM),a new functional monomer,was prepared by hydrolysis of maleic anhydride(MA) followed by acid-catalyzed addition reaction with dicyclopentadiene(DCPD),and the yield of DHCM was up to 90% with its purity exceeding 85%.The molecular structure of product was characterized by EA,FT-IR spectroscopy and GC-MS,and the synthetic technology and performance of DHCM were also studied.
Keywords:dicyclopentadiene monomaleate  synthesis  dicyclopentadiene  maleic anhydride
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