| 原甲酸三乙酯合成新工艺 |
| |
| 引用本文： | 崔学元,金长荣.原甲酸三乙酯合成新工艺[J].江苏化工,1996,24(5):26-27,43. |
| |
| 作者姓名： | 崔学元 金长荣 |
| |
| 作者单位： | 锦西化工总厂研究所!葫芦岛，125001，锦西化工总厂研究所!葫芦岛，125001 |
| |
| 摘 要： | 介绍了以氯仿、乙醇、烧碱为原料，经一次反应制备原甲酸三乙酯的工艺。讨论了各种因素对反应的影响，得出了最佳工艺条件。产品纯度在９６％以上，产率可达４５％以上。该工艺具有成本低，操作简单易行等优点。
|
| 关 键 词： | 甲酸三乙酯 乙氧基甲烷 工艺 |
NEW TECHNOLOGY FOR SYNTHESIS OF TRIETHYL ORTHOFORMATE |
| |
| Cui Xueyuan and Jin Changrong.NEW TECHNOLOGY FOR SYNTHESIS OF TRIETHYL ORTHOFORMATE[J].Jiangsu Chemical Industry,1996,24(5):26-27,43. |
| |
| Authors: | Cui Xueyuan and Jin Changrong |
| |
| Abstract: | The technology for synthesizing triethyl orthoformate through primary reaction by taking chloroform,ethanol and caustic alkali as raw materials was reviewed. Effect of various factors on reaction were discussed. The optimum lechnological condition with more than 96% of purity of the product and more than 45% of yield was obtained. The technology has some advantages such as low cost and simiplicity of operation |
| |
| Keywords: | triethyl orthefermate chloform ethanol caustic alkali synthesis |
| 本文献已被 CNKI 维普 等数据库收录！ |
