Effect of inclusion size on mechanical properties of alumina toughened cubic zirconia |
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Authors: | Email author" target="_blank">Miros?aw?M?Bu?koEmail author Waldemar?Pyda |
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Affiliation: | (1) Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Mickiewicza Av. 30, 30-059 Cracow, Poland |
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Abstract: | The relationship between alumina inclusion size and mechanical properties of particulate cubic zirconia-alumina composites
was studied. The composites of the diverse size and content of alumina inclusions and of the nearly constant size of zirconia
grains were used. Physical mixtures of the 8 mol% Y2O3-ZrO2 nano-powder and the γ-Al2O3 or α -Al2O3 micro-powder were cold isostatically pressed and then pressurelessly sintered for 2 h at 1300∘C in air. The γ -Al2O3 and α -Al2O3 powder was composed of the particles of 0.17 and 0.36 μ m in size, respectively. Crystallites of the zirconia powder had
the size of 6 nm. Microstructural features of the composites have been characterised quantitatively. Hardness, critical stress
intensity factor and bending strength of the composites was measured and correlated with the microstructural features. Depending
on the size and content, the alumina inclusions influenced strength of the composites by influencing their fracture toughness
and the presence of flaws of critical size. An increase in size of the alumina inclusions was accompanied by the increase
of fracture toughness due to the additional contribution of large alumina inclusions to the crack deflection mechanism. It
was found that decreasing the alumina inclusion size significantly below the cubic zirconia matrix grain size (more than 3
times) did not lead to the increased values of fracture toughness of the composites. The highest increase in fracture toughness
(up to 3.9 MPa⋅ m0.5) has been found when the inclusion size was comparable to the matrix grain size. |
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