| 2-噻吩乙胺合成新工艺 |
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| 引用本文： | 邢俊德,宋志勇,苗茂谦,卢建军,张照昱.2-噻吩乙胺合成新工艺[J].化学世界,2013(11):663-665. |
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| 作者姓名： | 邢俊德 宋志勇 苗茂谦 卢建军 张照昱 |
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| 作者单位： | 太原理工大学化学化工学院;太原理工大学教育部与山西省煤科学与技术重点实验室 |
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| 摘 要： | 2-噻吩乙醇用SiO2负载的PCC(氯铬酸吡啶)氧化得2-噻吩乙醛,不经提纯,进一步与盐酸羟胺反应得2-噻吩乙醛肟,最后经NaBH4/CuSO4)/amberlyst-15还原得2-噻吩乙胺,总收率76.5%。
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| 关 键 词： | 2-噻吩乙胺 合成 2-噻吩乙醇 2-噻吩乙醛 2-噻吩乙醛肟 |
New Synthesis Process of 2-Thiopheneethylamine |
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| XING Jun-de;SONG Zhi-yong;MIAO Mao-qian;LU Jian-jun;ZHANG Zhao-yu.New Synthesis Process of 2-Thiopheneethylamine[J].Chemical World,2013(11):663-665. |
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| Authors: | XING Jun-de;SONG Zhi-yong;MIAO Mao-qian;LU Jian-jun;ZHANG Zhao-yu |
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| Affiliation: | XING Jun-de;SONG Zhi-yong;MIAO Mao-qian;LU Jian-jun;ZHANG Zhao-yu;Taiyuan University of Technology,College of Chemisty and Chemical Engineering;Key Laboratory of Coal Science and Technology,Ministry of Education and Shanxi Province; |
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