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组合桨聚合釜内非牛顿流体的混合特性
引用本文:包雨云,刘新卫,高正明,施力田,郑国军. 组合桨聚合釜内非牛顿流体的混合特性[J]. 合成橡胶工业, 2004, 27(3): 142-145
作者姓名:包雨云  刘新卫  高正明  施力田  郑国军
作者单位:北京化工大学,化学工程学院,北京,100029;北京化工大学,机电工程学院,北京,100029;北京燕山石油化工股份有限公司,合成橡胶事业部,北京,102503
摘    要:在φ476mm的椭圆底有机玻璃聚合釜中,以羧甲基纤维素-甘油水溶液(前者质量分数为1.3%)为实验物系。利用酸碱中和法测定了9种不同的搅拌桨直径与聚合釜直径比接近于1的组合搅拌桨沿聚合釜轴向及径向的混合特性。结果表明:内外螺带-锚式组合桨的轴向混合最强,但径向混合较差。框板式搅拌桨的轴向混合较内外螺带-锚式组合桨弱,但比改进偏框式桨强,其径向混合较后者弱。改进偏框桨的7种不同组合方式沿径向的混合良好,多数组合桨沿轴向的混合较前2种组合桨弱,更接近于平推流。

关 键 词:羧甲基纤维素-甘油水溶液  改进偏框组合桨  内外螺带-锚式组合桨  框板式搅拌桨  聚合釜  混合时间
文章编号:1000-1255(2004)03-0142-04

Mixing performance of agitators in a polymerization reactor with non-Newtonian fluid
Bao Yuyun ,Liu Xinwei ,Gao Zhengming ,Shi Litian ,Zheng Guojun. Mixing performance of agitators in a polymerization reactor with non-Newtonian fluid[J]. China Synthetic Rubber Industry, 2004, 27(3): 142-145
Authors:Bao Yuyun   Liu Xinwei   Gao Zhengming   Shi Litian   Zheng Guojun
Affiliation:Bao Yuyun 1,Liu Xinwei 2,Gao Zhengming 1,Shi Litian 1,Zheng Guojun 3
Abstract:In a cylindrical polymerization re actor of 0.476m diameter with elliptical bottom and no baffle,axial and radial mixing times were measured by using a decolourization method.Nine agitator configuratio ns including helical ribbon -anchor agitator,traditional frame -plate impeller and 7mod-ified asymmetric frame impellers we re used in the experi-ments.A non -Newtonian carboxymeth yl cellulose(CMC)-glycerin water solution was used as e xperimental liquid,the mass fraction of CMC was 1.3%.The results showed that he-lical ribbon -anchor agitator offered the shortest axial mixingtime and the longest radial mixing time among the nine agita-tors.Traditional frame -plate impeller had a medium axial and radial mixing performance.Most com binations of modified asymmetric frame impellers had much shorter radial mixing times and much longer axial mixing times than those of the former two agitators,more similar with the piston flow.
Keywords:carboxymethyl cellulose -glycerin water solu-tion  modified asymmetric frame imp eller  helical ribbon -an-chor agitator  frame -plate impelle r  polymerization reactor  mixing time
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