| 直接法合成甲基氯硅烷反应启动的研究 |
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| 引用本文： | 赵岩涛,崔华,李波,崔丽.直接法合成甲基氯硅烷反应启动的研究[J].弹性体,2010,20(4). |
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| 作者姓名： | 赵岩涛 崔华 李波 崔丽 |
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| 作者单位： | 中国石油吉林石化公司电石厂 中国石油吉林石化公司法律事务处 中国石油吉林石化公司建修公司 |
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| 基金项目： | 中国石油吉林石化分公司重点技术攻关项目 |
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| 摘 要： | 阐述了在流化床反应器中,氯甲烷气体和硅粉颗粒进行气固相反应,直接合成甲基氯硅烷的生产原理,及反应过程中反应诱导期(推料升温催化剂还原期)的工艺过程和反应机理。详细描述了反应诱导期的4个工艺过程:原料硅粉的准备;反应系统的确认;赶潮、推料、升温及流化床的改通,最后提出了发展建议。
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| 关 键 词： | 直接合成法 甲基氯硅烷 反应诱导期 引发 |
The research of startup during the direct synthesis reaction of methlchlorosilance |
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| ZHAO Yan-tao,CUI Hua,LI Bo,CUI Li.The research of startup during the direct synthesis reaction of methlchlorosilance[J].China Elastomerics,2010,20(4). |
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| Authors: | ZHAO Yan-tao CUI Hua LI Bo CUI Li |
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| Affiliation: | 1.The Calcium Carbide Factory of Jilin Petrochemical Co.Ltd.; PetroChina; Jilin 132022; China; 2.Legal Affairs Department; Jilin Petrochemical Co.Ltd.; 3 Construction Maintenance Company of Jilin Petrochemical Co.Ltd.; Jilin 132021; China); |
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| Abstract: | This paper expounded in a fluidized bed reactor,the chemical reaction between chlorosilane gas and grain of silicon powder,the theory of direct synthesis dimethyl dichlorosilane and the induction period process engineering and reaction mechanism.Detailed the four processes of the reaction induction period,which include:1.Preparing of raw material silicon powder,2.confirming the order reaction system,3.drying,pushing,rising temperature,4.Changing through fluidized bed.Finally,put forward the development prop... |
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| Keywords: | direct synthesis methlchlorosilance reaction induction period initiate |
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